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Extra info for Advances in Surface Science
Phys. Rev. B60, 9010 (1999), 9 1999, The American Physical Society. R-factor analysis on the basis of Pendry, Rp, or modified Zanazzi and Jona, RM~ is usually successfully applied [84, 85]. The results of the LEED experiments and calculations in comparison with a theoretical estimate are summarized in Table II. The structural parameters are defined in Figure 20 . The SURFACE CHARACTERIZATION: STRUCTURE AND TOPOGRAPHY TABLE II. ) ....... Parameter Au3Pd(110)LEED Au3Pd(110) sim. 07/~ not calc.
9 . _............. 0 _ . 6 ~ \ J\ N , ~ ~ _ ~ - - ~ __ 100 200 ,. 300 400 0 . 2 . 1 . , ~ _ . 9. 7 _ 500 Energy [eV] FIG. 14. The He + LEIS spectra from an A1203 surface covered with approximately one monolayer of Rh . Reprinted with permission from E. , 9 1997. some delay, also the O and A1 peaks. After some sputtering the Rh peak decreases again, whereas the O and A1 peak become stationary. The interpretation of such spectra is straight forward. Initially the surface including the Rh is covered with oxygen.
There it is assumed that the background intensity at one point is proportional to the intensity of the total peak area above the background and the integration constant is chosen to match the background at lower kinetic energies. This purely mathematical method is widely used because of its simple implementation and it has the advantage that it is independent of the choice of starting points. However, it has been shown that errors of typically 10-50% in the quantitative result are possible .
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