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Extra resources for Inorganic Mass Spectrometry: Fundamentals and Applications
Sample text
5 A in the fully oxidized P side ubiquinol oxidase N side Figure 1. ' ? 62 /Functional and Structural Analo gs of the Dioxygen Reduction Site in Terminal Oxidases Figure 2. " Electrons are transferred from ferrocytoch rome c to the binucl ear CUA site, to heme a and fin all y to the heme aJiCuB site w here O 2 is reduced. O 2 redu ctio n is coupled to translocation of 4 H + from the N side to the P site of the memb rane. His290 " .......... - .......... - ('"'\ L Figure 3. " two- subunit POX. II The variations in the intermetallic sepa ration is mo st likely du e to different ligation of the binuclear site.
2. Solid State Structural Studies. . . . . . . . . . . . . . . . . . . . . . . . . 3. Chemical and Electronic Properties. . . . . . . . . . . . . . . . . . . . . . .. E. Carbon Monoxide Adducts of (por)Fe"/Cu' Systems . . . . . . . . . . . . . . . . . .. 1. Synthesis. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2. Chemical and Spectroscopic Properties.
59 Such (LN)CuIlCN salts are readily made by metathesis of the appropriate (LN)CuIlCI complex with NaCN or KCN in methanolic solvent mixtures. 2. Solid State Structural Studies Single crystal X-ray diffraction structures have been determined for 14 cyanide bridged (por)Fe/Cu(L N) systems (Figure 6). Eleven of these structures concern modeling the fully oxidized (Felli/Cull) state, two are FellI/CuI systems and the remaining case is a fully reduced Fell/CuI derivative. 98 A) and Fe-C-N is essentially linear.
